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Mechanical evaluation of TiO_2-gritblasted and Ca-P magnetron sputter coated implants in goats

机译:山羊用TiO_2喷砂和Ca-P磁控溅射涂层植入物的力学性能评估

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Our aim was to evaluate the mechanical bone anchorage of TiO_2-gritblasted titanium implants as received (Ti) or provided with a calciumphosphate (Ca-P) coating of 0.1 mu m (CaP-0.1), 1 mu m (CaP-1), or 4 mu m (CaP-4) thickness. The implants were inserted in the femoral condyle of 12 goats. After 6 and 12 weeks, interface strength and appearance was evaluated using torque testing and scanning electron microscopy (SEM). Alreday at 6 weeks, all implants resisted very high torsional failure forces (Ti=117 Nm, CaP-0.1=142 Nm, CaP-1=154 Nm, and CaP-4=150 Nm). Although, CaP coated implants showed higher torque failure loads than noncoated implants, no statistical difference existed. The 12 week data (Ti=154 Nm, CaP-0.1=159 Nm, CaP-1=140 Nm, and CaP-4=171 Nm) demonstrated again no significant differences. Nevertheless, SEM showed that CaP-coated implants conducted more bone growth into the screwthreads. The fracture plane for CaP-4 implants was situated at the coating-implant interface or inside the coating. For CaP-0.1, CaP-1, and Ti implants, torque testing tesulted in failure at the bone-implant interface. Therefore, we conclude that all implants dresulted in a good bone bonding strength. The Ca-P coatings showed no negative initial effect, but seemed to improve the bone fixation.
机译:我们的目的是评估TiO_2喷砂处理的钛植入物(Ti)或提供有0.1μm(CaP-0.1),1μm(CaP-1)的磷酸钙(Ca-P)涂层的机械骨锚固性,或4微米(CaP-4)厚度。将植入物插入12只山羊的股骨dy中。 6和12周后,使用扭矩测试和扫描电子显微镜(SEM)评估界面强度和外观。在第6周的一天,所有植入物都抵抗非常高的扭转破坏力(Ti = 117 Nm,CaP-0.1 = 142 Nm,CaP-1 = 154 Nm和CaP-4 = 150 Nm)。尽管CaP涂层植入物显示出比未涂层植入物更高的扭矩破坏负荷,但没有统计学差异。 12周的数据(Ti = 154 Nm,CaP-0.1 = 159 Nm,CaP-1 = 140 Nm和CaP-4 = 171 Nm)再次没有显着差异。尽管如此,SEM显示,CaP涂层植入物使更多的骨骼生长进入螺纹。 CaP-4植入物的骨折平面位于涂层-植入物界面或涂层内部。对于CaP-0.1,CaP-1和Ti植入物,扭矩测试导致了骨-植入物界面的破坏。因此,我们得出结论,所有植入物都具有良好的骨结合强度。 Ca-P涂层没有显示出负面的初始效果,但似乎可以改善骨骼的固定。

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