Micro-coiled carbon fibers were prepared by catalytic pyrolysis ofacetylene with nano- sized nickel powder catalyst using the substratemethod. The morphology of micro-coiled carbon fibers was observedthrough field emission scanning electron microscopy. It was foundthat the fiber and coil diameter of the obtained micro-coiled carbonfibers is about 500-600 nm and 4-5 μm, respectively.
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